A Simple Method for Preparation of Nano-sized ZnO
ثبت نشده
چکیده
Nano is an advanced technology which in recent years has had numerous applications in different fields such as industry, biotechnology, energy, environment and etc. In this paper, ZnO nanoparticles were synthesized by simple method of precipitation sounds more plausible. ZnSO4 and NH4OH were used as precursors to yield ZnO powders. The synthesized ZnO nanoparticles were characterized by X-ray diffraction measurements (XRD), scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDX). According to the results of XRD analysis, the purity of ZnO nanoparticles was obtained; based on the William-Hal method, the mean size of particles was achieved equal to 30 nm. This test has also shown the high crystallinity of the ZnO nanoparticles. As SEM analysis revealed, the morphology of ZnO nanoparticles to be flake like shapes with the mean particle size of 30 nm. Finally, the analysis of the synthesized nano sample by using percentage of EDX has indicated that the purity of ZnO was quite high. Received date: 27/04/2016 Accepted date: 17/06/2016 Published date: 22/06/2016
منابع مشابه
Preparation of ZnO-Polystyerne Composite Films and Investigation of Antibacterial Properties of ZnO-Polystyerne Composite Films
Background & Objectives: Nanotechnology is one of great important part of technology. Nanoparticles can be used in different applications for industrial, medical, military and personal use. The objectives of this study were preparation of Polystyrene/ZnO nanocomposite films via a simple method and investigation of antibacterial activity of them. Methods: Polystyrene /ZnO nanoparticle (PS/nano-...
متن کاملSonochemical Synthesis and Characterization of a Nano-Sized Lead (II) Coordination Polymer; A New Precursor for the Preparation of PbO Nanoparticles
Development of components that can form large molecular aggregates through non–covalent interactions, in nano size structures, has been an active area of research. In current study, a nano-sized Pb(II) coordination polymer, {[Pb(pydc)(pydc.H2)(H2O)2]2}n (1), where [pydc.H2= 2,6-pyridinedicarboxylic acid), wer...
متن کاملSynthesis and Characterization of Nano-Sized Hexagonal and Spherical Nanoparticles of Zinc Oxide
ZnO plays an important role in many semiconductors technological aspects. Here, direct precipitation method was employed for the synthesis of nano-sized hexagonal ZnO particles, which is based on chemical reactions between raw materials used in the experiment. ZnO nanoparticles were synthesized by calcinations of the ZnO precursor precipitates at 250 ˚C for 3hours. ...
متن کاملSonochemical synthesis and characterization of nano-sized zinc(II) coordination complex as a precursor for the preparation of pure-phase zinc(II) oxide nanoparticles
In current study, nanoparticles and single crystals of a Zn(II) coordination complex, [Zn(dmph)I2](1), {dmph=2,9-dimethyl-1,10-phenanthroline(neocuproine)}, have been synthesized by the reaction of zinc(II) acetate, KI and neocuproine as ligand in methanol using sonochemical and heat gradient methods, respectively. The nanostructure of 1 was characte...
متن کاملEnhancement of photocatalytic activity of ZnO–SiO2 by nano-sized Pt for efficient removal of dyes from wastewater effluents
In this work, ZnO/SiO2 nanoparticles were prepared using sol-gel method, and platinum particles were loaded on ZnO/SiO2 nanoparticles by photoreductive method. Samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and Fourier transform infrared spectroscopy (FT-IR). The XRD patterns showed that the zinc oxide samples have a wurtzite structure (hexagonal phase...
متن کامل